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Gel Manufacturing: SOP for Visual Inspection of Filled Gel Tubes – V 2.0

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Gel Manufacturing: SOP for Visual Inspection of Filled Gel Tubes – V 2.0

Standard Operating Procedure for Visual Inspection of Filled Gel Tubes in Gel Manufacturing


Department Gel Manufacturing
SOP No. SOP/GM/116/2025
Supersedes SOP/GM/116/2022
Page No. Page 1 of 10
Issue Date 02/06/2025
Effective Date 04/06/2025
Review Date 02/06/2027

1. Purpose

To lay down the procedure for performing visual inspection of filled gel tubes for identifying any cosmetic or critical defects prior to secondary packaging.

2. Scope

This procedure applies to all batches of gel formulations filled in collapsible or laminated tubes in the gel

manufacturing department.

3. Responsibilities

  • Production Operator: Conducts visual inspection as per training and defect identification criteria.
  • Production Supervisor: Ensures process adherence and documents inspection records.
  • QA Inspector: Performs periodic verification and line clearance post-inspection.
See also  Gel Manufacturing: SOP for Conducting Photostability Testing for Gels - V 2.0

4. Accountability

Head – Manufacturing

5. Procedure

5.1 Preparation for Visual Inspection

  1. Inspectors must be trained in defect identification and visual acuity testing must be valid.
  2. Set up visual inspection booth with uniform white lighting (~1000 Lux) and black/white background.
  3. Ensure cleanliness of inspection area, bench, gloves, and collection trays.

5.2 Defect Categories

Defects are classified as follows:

  • Critical: Broken seal, leakage, contamination, improper closure.
  • Major: Improper labeling, dented/crushed tube, offset printing.
  • Minor: Smudging, slight variation in crimp, cosmetic scuff marks.

5.3 Execution of Visual Inspection

  1. Collect filled tubes post-crimping and organize in inspection trays.
  2. Inspect each tube against white and black backgrounds under light.
  3. Rotate tubes to observe 360° surface and crimp integrity.
  4. Segregate defective tubes into designated rejection bins based on defect type.
  5. Record number of inspected and rejected units in the inspection logbook.
See also  Gel Manufacturing: SOP for Weighing Micro Quantities of APIs for Gels - V 2.0

5.4 Reconciliation and Review

  1. After inspection, reconcile the number of accepted and rejected units.
  2. Generate summary report showing defect trends and batch defect rate.
  3. Submit report to QA for batch record compilation.

6. Abbreviations

  • QA: Quality Assurance
  • Lux: Unit of illumination
  • SOP: Standard Operating Procedure

7. Documents

  1. Visual Inspection Checklist – Annexure-1
  2. Defect Reference Chart – Annexure-2
  3. Inspection Logbook – Annexure-3

8. References

  • WHO TRS 961 Annex 3: GMP for Pharmaceutical Products
  • FDA Guidance on Visual Inspection of Drug Products

9. SOP Version

Version: 2.0

10. Approval Section

Prepared By Checked By Approved By
Signature
Date
Name
Designation Jr. Production Chemist QA Executive Head – Manufacturing
Department Gel Manufacturing Quality Assurance Manufacturing
See also  Gel Manufacturing: SOP for Labeling and Coding of Gel Products Before Secondary Packing - V 2.0

11. Annexures

Annexure-1: Visual Inspection Checklist

Parameter Yes/No Remarks
Seal Intact
Proper Label
Tube Body Free from Defect
Batch Code & Mfg. Date Present

Annexure-2: Defect Reference Chart

Defect Type Image Reference Category
Cracked Cap DRC-01 Critical
Printing Misalignment DRC-02 Major
Scuff Marks DRC-03 Minor

Annexure-3: Inspection Logbook Format

Date Batch No. No. of Tubes Inspected No. of Defects Remarks Inspector

Revision History

Revision Date Revision No. Change Description Reason Approved By
28/08/2022 1.0 Initial SOP New SOP QA Head
02/06/2025 2.0 Updated inspection parameters and annexures Annual Review QA Head
Gels V 2.0 Tags:gel excipients SOP, gel extrudability SOP, gel formulation process guidelines, gel formulation safety SOP, gel formulation SOP template, gel homogenization SOP, gel ingredient weighing SOP, gel labeling and documentation SOP, gel microbial contamination SOP, gel packaging SOP, gel viscosity measurement SOP, gel viscosity testing SOP, pharmaceutical gel SOP, quality control SOP gel formulations, SOP for carbopol gel formulation, SOP for gel pH adjustment, SOP for gel spreadability test, stability testing SOP gel, standard operating procedure gel preparation, topical gel manufacturing SOP

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Standard Operating Procedures V 1.0

  • Aerosols
  • Analytical Method Development
  • Bioequivalence Bioavailability Study
  • Capsule Formulation
  • Clinical Studies
  • Creams
  • Data Integrity
  • Dental Dosage Forms
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  • Maintenance Dept.
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  • Pharmacovigilance
  • Powder & Granules
  • Purchase Departments
  • Quality Assurance
  • Quality Control
  • Raw Material Stores
  • Regulatory Affairs
  • Tablet Manufacturing
  • Rectal Dosage Forms
  • Transdermal Patches
  • Vaginal Dosage Forms
  • Validations and Qualifications

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NEW! Revised SOPs – V 2.0

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  • BA-BE Studies V 2.0
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