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Elixir Department: SOP for Agitator Blade Changeover Procedure – V 2.0

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Elixir Department: SOP for Agitator Blade Changeover Procedure – V 2.0

Standard Operating Procedure for Agitator Blade Changeover in Elixir Manufacturing

Department Elixir Department
SOP No. SOP/ELX/106/2025
Supersedes SOP/ELX/106/2022
Page No. Page 1 of 8
Issue Date 11/04/2025
Effective Date 15/04/2025
Review Date 11/04/2026

1. Purpose

To establish a standard method for safely changing and verifying agitator blades in mixing vessels used for elixir manufacturing, depending on the type of product and process requirements.

2. Scope

This SOP applies to all changeover activities involving agitator blades for variable-speed and fixed-speed mixers in the Elixir Department.

3. Responsibilities

  • Maintenance Technician:
    • Perform changeover and verify secure installation of blades.
  • Production Operator:
    • Support blade changeover and ensure equipment is ready for use.
  • Production Supervisor:
    • Authorize blade changeover and inspect post-installation alignment.
  • QA Officer:
    • Verify and approve equipment status before batch startup.

4. Accountability

The Head of Engineering and Head of Production are jointly accountable for proper changeover and preventive maintenance of agitator blades and ensuring safe operation.

See also  Elixir Department: SOP for Identification and Labeling of Clean Equipment - V 2.0

5. Procedure

5.1 Prerequisites

  1. Refer to the batch-specific process parameters to confirm if blade changeover is required (e.g.,
from paddle to turbine type).
  • Ensure the mixing vessel is cleaned and labeled “UNDER MAINTENANCE.”
  • Verify that the agitator motor is turned off and LOTO (Lockout/Tagout) is applied.
  • 5.2 Removal of Existing Blade

    1. Wear appropriate PPE (gloves, goggles, safety shoes).
    2. Loosen the blade locking mechanism using the appropriate tool (e.g., wrench or torque spanner).
    3. Gently slide or unbolt the blade from the shaft and place it in a designated tray.
    4. Inspect the shaft and blade area for corrosion, cracks, or deformation.

    5.3 Installation of New Blade

    1. Select the required blade type as per process specification (e.g., anchor, propeller, turbine).
    2. Visually inspect the new blade for cleanliness and physical integrity.
    3. Align the blade with the agitator shaft and secure it using the locking mechanism or bolts provided.
    4. Ensure that the blade is firmly fixed and centered.

    5.4 Verification and Trial Run

    1. Remove all tools and confirm the work area is clear.
    2. Remove the LOTO tag and restore power supply.
    3. Run the agitator on minimum RPM for 30 seconds and observe for any abnormal noise or vibration.
    4. If acceptable, increase to working RPM and check for stability.
    5. Record observations in the Blade Changeover Log (Annexure-1).

    5.5 Post-Changeover Activities

    1. Update the equipment status label to “READY FOR USE.”
    2. Production Supervisor to verify installation and sign off in the logbook.
    3. QA to review records before batch initiation.

    6. Abbreviations

    • SOP: Standard Operating Procedure
    • QA: Quality Assurance
    • LOTO: Lockout Tagout
    • PPE: Personal Protective Equipment

    7. Documents

    1. Blade Changeover Log (Annexure-1)
    2. Equipment Maintenance Log
    3. Batch Manufacturing Record (BMR)

    8. References

    • WHO TRS 1010 – GMP Guidelines for Equipment
    • 21 CFR Part 211.67 – Maintenance of Equipment
    • OEM Manuals of Agitators

    9. SOP Version

    Version: 2.0

    10. Approval Section

    Prepared By Checked By Approved By
    Signature
    Date
    Name
    Designation
    Department

    11. Annexures

    Annexure-1: Blade Changeover Log

    Date Equipment ID Old Blade Type New Blade Type Reason for Change Technician Supervisor
    11/04/2025 MIX-104 Turbine Anchor High Viscosity Batch Rajesh Kumar Sunita Reddy

    Revision History:

    Revision Date Revision No. Revision Details Reason for Revision Approved By
    01/01/2024 1.0 Initial SOP Release New SOP QA Head
    11/04/2025 2.0 Included trial run step and blade type specification Process Safety Enhancement QA Head
    See also  Elixir Department: SOP for Handling Overages in Batch Preparation - V 2.0
    Elixers V 2.0 Tags:Elixir colorants, Elixir dosage form, Elixir filtration techniques, Elixir flavoring agents, Elixir formulation, Elixir GMP compliance, Elixir manufacturing process, Elixir manufacturing SOPs, Elixir packaging requirements, Elixir pharmacopoeial standards, Elixir preparation methods, Elixir preservatives, Elixir production equipment, Elixir quality control, Elixir regulatory guidelines, Elixir shelf life, Elixir stability testing, Elixir sterilization methods, Elixir storage conditions, Elixir sweetening agents, Elixir viscosity modifiers, Hydroalcoholic solutions, Medicated elixirs, Non-medicated elixirs, Pharmaceutical elixirs

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    Standard Operating Procedures V 1.0

    • Aerosols
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    NEW! Revised SOPs – V 2.0

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